Kuhlmann, Christopher: Optimization and application of flowing atmospheric-pressure afterglow mass spectrometry for direct surface sampling and quantitative analysis. 2019
Inhalt
- Title page
- Abstract
- Zusammenfassung
- Table of Content
- 1 Introduction and Scope of the Thesis
- 2 Optimization of Plasma-Based Ambient Desorption/Ionization Mass Spectrometry Operating Parameters
- 2.1 Introduction
- 2.2 Instrumental Modifications of the ADI Source Design
- 2.3 Important Parameters to Improve the Analyte Desorption by Plasma-Based ADI Sources
- 2.4 Parameters for the Adjustment of the Analyte Ionization Process
- 2.5 Sample Probes and Substrates for Plasma-Based ADI-MS of Liquid Samples
- 2.6 Modifications of the MS Interface for Improved ADI-MS Sensitivity
- 2.7 Conclusion
- 3 Optimization of the Flowing Atmospheric-Pressure Afterglow Plasma-Source Geometry and Development of a Temperature-Controlled Sample Holder for Direct Mass Spectral Surface Analysis
- 4 Plasma-Based Ambient Desorption/Ionization Mass Spectrometry for the Analysis of Liquid Crystals Employed in Display Devices
- 5 Spatially-Resolved Analysis of Liquid Crystals in Liquid Crystal Display Test Cells via Flowing Atmospheric-Pressure Afterglow Mass Spectrometry
- 6 Fast Screening and Quantitative Mass Spectral Imaging of Thin-Layer Chromatography Plates with Flowing Atmospheric-Pressure Afterglow High-Resolution Mass Spectrometry
- 7 High-Performance Thin-Layer Chromatography Flowing Atmospheric-Pressure Afterglow Mass Spectrometry for Fast Antimalarial Agent Screening in Drug Tablets
- 8 Decomposition of P4O10 in DMSO
- 9 Concluding Remarks and Future Perspectives
- 10 References
- 11 Appendix
- 11.1 Mass Spectrometer Operating Conditions for ADI-MS
- 11.2 IR-Thermography
- 11.3 Data Evaluation Procedure for Transient Signals
- 11.4 Data Evaluation Procedure for Mass Spectral Imaging
- 11.5 Data Evaluation Procedure for the Determination of Instrumental Detection Limits Measured with High-Resolution Mass Spectrometry
- 11.6 Supporting Information for the Analysis of Lithium-Ion Batteries
- 11.7 Supporting Information for the Analysis of Liquid Crystals via Plasma-Based ADI-MS
- 11.8 Supporting Information for Spatially-Resolved Liquid Crystal Analysis via FAPA-MS and LA-h-FAPA-MS
- 11.9 Supporting Information for the Analysis of TLC plates via FAPA-MS
- 11.10 Supporting Information for the Analysis of Antimalarial Agent Screening via HPTLC-FAPA-MS
- 12 Abbreviations
- 13 List of Figures
- 14 List of Tables
- 15 Acknowledgements
- 17 List of Publications