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Introduction"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636890","https://noah.nrw/i3f/v20/3559684/canvas/3636891","https://noah.nrw/i3f/v20/3559684/canvas/3636892","https://noah.nrw/i3f/v20/3559684/canvas/3636893","https://noah.nrw/i3f/v20/3559684/canvas/3636894","https://noah.nrw/i3f/v20/3559684/canvas/3636895","https://noah.nrw/i3f/v20/3559684/canvas/3636897","https://noah.nrw/i3f/v20/3559684/canvas/3636898","https://noah.nrw/i3f/v20/3559684/canvas/3636899","https://noah.nrw/i3f/v20/3559684/canvas/3636900","https://noah.nrw/i3f/v20/3559684/canvas/3636901","https://noah.nrw/i3f/v20/3559684/canvas/3636903","https://noah.nrw/i3f/v20/3559684/canvas/3636904","https://noah.nrw/i3f/v20/3559684/canvas/3636905","https://noah.nrw/i3f/v20/3559684/canvas/3636907","https://noah.nrw/i3f/v20/3559684/canvas/3636908","https://noah.nrw/i3f/v20/3559684/canvas/3636910","https://noah.nrw/i3f/v20/3559684/canvas/3636911","https://noah.nrw/i3f/v20/3559684/canvas/3636913","https://noah.nrw/i3f/v20/3559684/canvas/3636914"],"ranges":["https://noah.nrw/i3f/v20/3559684/range/3636889","https://noah.nrw/i3f/v20/3559684/range/3636896","https://noah.nrw/i3f/v20/3559684/range/3636902","https://noah.nrw/i3f/v20/3559684/range/3636906","https://noah.nrw/i3f/v20/3559684/range/3636909","https://noah.nrw/i3f/v20/3559684/range/3636912"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636888","@type":"sc:Range","label":"2. Glass Transition Temperature and Viscoelastic Behavior of Polymers"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636890","https://noah.nrw/i3f/v20/3559684/canvas/3636891","https://noah.nrw/i3f/v20/3559684/canvas/3636892","https://noah.nrw/i3f/v20/3559684/canvas/3636893","https://noah.nrw/i3f/v20/3559684/canvas/3636894","https://noah.nrw/i3f/v20/3559684/canvas/3636895"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636889","@type":"sc:Range","label":"2.1. The glass transition temperature Tg"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636897","https://noah.nrw/i3f/v20/3559684/canvas/3636898","https://noah.nrw/i3f/v20/3559684/canvas/3636899","https://noah.nrw/i3f/v20/3559684/canvas/3636900","https://noah.nrw/i3f/v20/3559684/canvas/3636901"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636896","@type":"sc:Range","label":"2.2. Viscoelastic properties of polymers"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636903","https://noah.nrw/i3f/v20/3559684/canvas/3636904","https://noah.nrw/i3f/v20/3559684/canvas/3636905"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636902","@type":"sc:Range","label":"2.3. Sub-Tg relaxations in polymers"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636907","https://noah.nrw/i3f/v20/3559684/canvas/3636908"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636906","@type":"sc:Range","label":"2.4. Determination of glass transition temperature"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636910","https://noah.nrw/i3f/v20/3559684/canvas/3636911"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636909","@type":"sc:Range","label":"2.5. Physical aging and cooling rate dependency of Tg"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636913","https://noah.nrw/i3f/v20/3559684/canvas/3636914"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636912","@type":"sc:Range","label":"2.6. 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Atomic Force Microscope (AFM)"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636918","https://noah.nrw/i3f/v20/3559684/canvas/3636919"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636917","@type":"sc:Range","label":"3.1 Fundamental principles of AFM"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636921","https://noah.nrw/i3f/v20/3559684/canvas/3636922","https://noah.nrw/i3f/v20/3559684/canvas/3636923","https://noah.nrw/i3f/v20/3559684/canvas/3636924","https://noah.nrw/i3f/v20/3559684/canvas/3636925","https://noah.nrw/i3f/v20/3559684/canvas/3636926"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636920","@type":"sc:Range","label":"3.2. AFM force-distance curves"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636928","https://noah.nrw/i3f/v20/3559684/canvas/3636929","https://noah.nrw/i3f/v20/3559684/canvas/3636930","https://noah.nrw/i3f/v20/3559684/canvas/3636931","https://noah.nrw/i3f/v20/3559684/canvas/3636932","https://noah.nrw/i3f/v20/3559684/canvas/3636933"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636927","@type":"sc:Range","label":"3.3. Analysis of contact regime"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636935","https://noah.nrw/i3f/v20/3559684/canvas/3636936","https://noah.nrw/i3f/v20/3559684/canvas/3636937","https://noah.nrw/i3f/v20/3559684/canvas/3636938","https://noah.nrw/i3f/v20/3559684/canvas/3636939","https://noah.nrw/i3f/v20/3559684/canvas/3636940"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636934","@type":"sc:Range","label":"3.4. Calibration"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636942","https://noah.nrw/i3f/v20/3559684/canvas/3636943"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636941","@type":"sc:Range","label":"3.5. Force volume measurements"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636946","https://noah.nrw/i3f/v20/3559684/canvas/3636948","https://noah.nrw/i3f/v20/3559684/canvas/3636951","https://noah.nrw/i3f/v20/3559684/canvas/3636952","https://noah.nrw/i3f/v20/3559684/canvas/3636954","https://noah.nrw/i3f/v20/3559684/canvas/3636956","https://noah.nrw/i3f/v20/3559684/canvas/3636957","https://noah.nrw/i3f/v20/3559684/canvas/3636958"],"ranges":["https://noah.nrw/i3f/v20/3559684/range/3636945","https://noah.nrw/i3f/v20/3559684/range/3636947","https://noah.nrw/i3f/v20/3559684/range/3636949","https://noah.nrw/i3f/v20/3559684/range/3636950","https://noah.nrw/i3f/v20/3559684/range/3636953","https://noah.nrw/i3f/v20/3559684/range/3636955"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636944","@type":"sc:Range","label":"4. Experimental Section"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636946"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636945","@type":"sc:Range","label":"4.1. Polymers and chemicals"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636948"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636947","@type":"sc:Range","label":"4.2. Preparation of polymer films from solutions"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636951","https://noah.nrw/i3f/v20/3559684/canvas/3636952"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636950","@type":"sc:Range","label":"4.4. AFM measurements"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636954"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636953","@type":"sc:Range","label":"4.5. Dynamic mechanical analysis"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636956","https://noah.nrw/i3f/v20/3559684/canvas/3636957","https://noah.nrw/i3f/v20/3559684/canvas/3636958"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636955","@type":"sc:Range","label":"4.6. Broadband spectroscopy"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636961","https://noah.nrw/i3f/v20/3559684/canvas/3636962","https://noah.nrw/i3f/v20/3559684/canvas/3636963","https://noah.nrw/i3f/v20/3559684/canvas/3636964","https://noah.nrw/i3f/v20/3559684/canvas/3636965","https://noah.nrw/i3f/v20/3559684/canvas/3636966","https://noah.nrw/i3f/v20/3559684/canvas/3636968","https://noah.nrw/i3f/v20/3559684/canvas/3636969","https://noah.nrw/i3f/v20/3559684/canvas/3636970","https://noah.nrw/i3f/v20/3559684/canvas/3636971","https://noah.nrw/i3f/v20/3559684/canvas/3636972","https://noah.nrw/i3f/v20/3559684/canvas/3636974","https://noah.nrw/i3f/v20/3559684/canvas/3636975","https://noah.nrw/i3f/v20/3559684/canvas/3636976","https://noah.nrw/i3f/v20/3559684/canvas/3636977","https://noah.nrw/i3f/v20/3559684/canvas/3636978","https://noah.nrw/i3f/v20/3559684/canvas/3636979","https://noah.nrw/i3f/v20/3559684/canvas/3636980","https://noah.nrw/i3f/v20/3559684/canvas/3636982","https://noah.nrw/i3f/v20/3559684/canvas/3636983","https://noah.nrw/i3f/v20/3559684/canvas/3636984","https://noah.nrw/i3f/v20/3559684/canvas/3636985","https://noah.nrw/i3f/v20/3559684/canvas/3636986","https://noah.nrw/i3f/v20/3559684/canvas/3636987","https://noah.nrw/i3f/v20/3559684/canvas/3636988","https://noah.nrw/i3f/v20/3559684/canvas/3636989","https://noah.nrw/i3f/v20/3559684/canvas/3636990"],"ranges":["https://noah.nrw/i3f/v20/3559684/range/3636960","https://noah.nrw/i3f/v20/3559684/range/3636967","https://noah.nrw/i3f/v20/3559684/range/3636973","https://noah.nrw/i3f/v20/3559684/range/3636981"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636959","@type":"sc:Range","label":"5. 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Hyperbolic fit"},{"canvases":["https://noah.nrw/i3f/v20/3559684/canvas/3636974","https://noah.nrw/i3f/v20/3559684/canvas/3636975","https://noah.nrw/i3f/v20/3559684/canvas/3636976","https://noah.nrw/i3f/v20/3559684/canvas/3636977","https://noah.nrw/i3f/v20/3559684/canvas/3636978","https://noah.nrw/i3f/v20/3559684/canvas/3636979","https://noah.nrw/i3f/v20/3559684/canvas/3636980"],"@id":"https://noah.nrw/i3f/v20/3559684/range/3636973","@type":"sc:Range","label":"5.3. 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